Information card for entry 7045696

Structure parameters

• Formula: C24 H22 Cl F3 N3 O5 Rh S
• Calculated formula: C24 H22 Cl F3 N3 O5 Rh S
• Title of publication: N-Heterotricyclic cationic carbene ligands. Synthesis, reactivity and coordination chemistry.
• Authors of publication: Iglesias-Sigüenza, Javier; Izquierdo, Cristina; Díez, Elena; Fernández, Rosario; Lassaletta, José M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 15
• Pages of publication: 5196 - 5206
• a: 7.6788 ± 0.0004 Å
• b: 23.8363 ± 0.0012 Å
• c: 14.9392 ± 0.0007 Å
• α: 90°
• β: 102.651 ± 0.002°
• γ: 90°
• Cell volume: 2668 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0568
• Weighted residual factors for significantly intense reflections: 0.1637
• Weighted residual factors for all reflections included in the refinement: 0.1777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.264
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No