Information card for entry 7045695

Structure parameters

• Formula: C33 H37 F6 N4 O6 Rh S2
• Calculated formula: C33 H37 F6 N4 O6 Rh S2
• Title of publication: N-Heterotricyclic cationic carbene ligands. Synthesis, reactivity and coordination chemistry.
• Authors of publication: Iglesias-Sigüenza, Javier; Izquierdo, Cristina; Díez, Elena; Fernández, Rosario; Lassaletta, José M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 15
• Pages of publication: 5196 - 5206
• a: 13.0101 ± 0.0007 Å
• b: 11.4324 ± 0.0006 Å
• c: 24.3136 ± 0.0013 Å
• α: 90°
• β: 100.037 ± 0.002°
• γ: 90°
• Cell volume: 3561 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1512
• Weighted residual factors for all reflections included in the refinement: 0.1619
• Goodness-of-fit parameter for all reflections included in the refinement: 1.321
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No