Information card for entry 7046336

Structure parameters

• Formula: C33 H35 Cu F6 N2 W
• Calculated formula: C33 H35 Cu F6 N2 W
• Title of publication: Preparation and characterisation of heterobimetallic copper-tungsten hydride complexes.
• Authors of publication: Hicken, Alexandra; White, Andrew J. P.; Crimmin, Mark R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 31
• Pages of publication: 10595 - 10600
• a: 20.6872 ± 0.0002 Å
• b: 21.27381 ± 0.00017 Å
• c: 15.15393 ± 0.00018 Å
• α: 90°
• β: 110.535 ± 0.0013°
• γ: 90°
• Cell volume: 6245.41 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0392
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0671
• Weighted residual factors for all reflections included in the refinement: 0.0726
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No