Information card for entry 7046337

Structure parameters

• Formula: C27 H19 Cu F10 N2 W
• Calculated formula: C27 H17 Cu F10 N2 W
• Title of publication: Preparation and characterisation of heterobimetallic copper-tungsten hydride complexes.
• Authors of publication: Hicken, Alexandra; White, Andrew J. P.; Crimmin, Mark R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 31
• Pages of publication: 10595 - 10600
• a: 7.5947 ± 0.0003 Å
• b: 17.2024 ± 0.0007 Å
• c: 20.5126 ± 0.001 Å
• α: 90°
• β: 98.831 ± 0.005°
• γ: 90°
• Cell volume: 2648.1 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0588
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.161
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No