Information card for entry 7046338

Structure parameters

• Formula: C36 H68 Cu2 Li2 Si4 W2
• Calculated formula: C36 H68 Cu2 Li2 Si4 W2
• Title of publication: Preparation and characterisation of heterobimetallic copper-tungsten hydride complexes.
• Authors of publication: Hicken, Alexandra; White, Andrew J. P.; Crimmin, Mark R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 31
• Pages of publication: 10595 - 10600
• a: 10.2525 ± 0.0005 Å
• b: 10.8355 ± 0.0007 Å
• c: 12.468 ± 0.0007 Å
• α: 67.095 ± 0.006°
• β: 72.887 ± 0.005°
• γ: 63.99 ± 0.006°
• Cell volume: 1133.8 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0297
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0669
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No