Information card for entry 7047227

Structure parameters

• Formula: C28 H54.05 Li2 N4 O2 P2
• Calculated formula: C28 H54.456 Li2 N4 O2 P2
• Title of publication: The chameleonic reactivity of dilithio bis(alkylamido)cyclodiphosph(iii)azanes with chlorophosphines.
• Authors of publication: Otang, Mathew E.; Josephson, David; Duppong, Todd; Stahl, Lothar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11625 - 11635
• a: 18.8882 ± 0.0006 Å
• b: 10.0899 ± 0.0003 Å
• c: 19.7056 ± 0.0006 Å
• α: 90°
• β: 118.019 ± 0.0009°
• γ: 90°
• Cell volume: 3315.32 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.94 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0623
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1279
• Weighted residual factors for all reflections included in the refinement: 0.1392
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No