Information card for entry 7049796

Structure parameters

• Formula: C65 H53 Cl3 Cu4 N12 O16
• Calculated formula: C65 H53 Cl3 Cu4 N12 O16
• Title of publication: Tetranuclear Mn^II, Co^II, Cu^II and Zn^II grid complexes of an unsymmetrical ditopic ligand: synthesis, structure, redox and magnetic properties.
• Authors of publication: Lakma, Avinash; Hossain, Sayed Muktar; van Leusen, Jan; Kögerler, Paul; Singh, Akhilesh Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 22
• Pages of publication: 7766 - 7777
• a: 17.691 ± 0.003 Å
• b: 25.597 ± 0.004 Å
• c: 14.797 ± 0.002 Å
• α: 90°
• β: 105.578 ± 0.005°
• γ: 90°
• Cell volume: 6454.5 ± 1.7 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0835
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.095
• Weighted residual factors for all reflections included in the refinement: 0.1101
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No