Information card for entry 7049797

Structure parameters

• Formula: C64 H52 N12 O16 Zn4
• Calculated formula: C64 H52 N12 O16 Zn4
• Title of publication: Tetranuclear Mn^II, Co^II, Cu^II and Zn^II grid complexes of an unsymmetrical ditopic ligand: synthesis, structure, redox and magnetic properties.
• Authors of publication: Lakma, Avinash; Hossain, Sayed Muktar; van Leusen, Jan; Kögerler, Paul; Singh, Akhilesh Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 22
• Pages of publication: 7766 - 7777
• a: 25.877 ± 0.0014 Å
• b: 12.4849 ± 0.0006 Å
• c: 20.9258 ± 0.0011 Å
• α: 90°
• β: 112.903 ± 0.002°
• γ: 90°
• Cell volume: 6227.6 ± 0.6 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.132
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1249
• Weighted residual factors for all reflections included in the refinement: 0.1585
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No