Information card for entry 7052341

Structure parameters

• Formula: C78 H72 Cl2 F20 N4 P4 Ru2 Sb2
• Calculated formula: C78 H72 Cl2 F20 N4 P4 Ru2 Sb2
• Title of publication: Imination reactions of free and coordinated 2-diphenylphosphino-1-phenyl-phospholane: Access to regioisomeric ruthenium(<small>II</small>) complexes containing novel iminophosphorane‒phosphine ligands
• Authors of publication: Alba E. Díaz-Álvarez; Pascale Crochet; Maria Zablocka; Victorio Cadierno; Carine Duhayon; José Gimeno; Jean-Pierre Majoral
• Journal of publication: New Journal of Chemistry
• Year of publication: 2006
• Journal volume: 30
• Journal issue: 9
• Pages of publication: 1295
• a: 9.2949 ± 0.0018 Å
• b: 12.576 ± 0.003 Å
• c: 18.412 ± 0.003 Å
• α: 101.298 ± 0.017°
• β: 90.983 ± 0.015°
• γ: 95.652 ± 0.017°
• Cell volume: 2098.8 ± 0.7 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.3028
• Residual factor for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections: 0.1228
• Weighted residual factors for significantly intense reflections: 0.0848
• Weighted residual factors for all reflections included in the refinement: 0.0848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No