Information card for entry 7053440

Structure parameters

• Common name: (Bis-(mu-2-4-(Diphenylphosphino)methyl-1,2-catecholato)-bis- (mu-2-3-(diphenylphosphino)methyl-hydro-1,2-catecholato)- (dimethylforamide)-yttrium(iii)) chloride dimethylformamide solvate
• Chemical name: [Bis-(mu-2-4-(Diphenylphosphino)methyl-1,2-catecholato)-bis-(mu-2-3- (diphenylphosphino)methyl-hydro-1,2-catecholato)-(dimethylforamide)- yttrium(III)] chloride dimethylformamide solvate
• Formula: C88 H90 Cl N4 O12 P4 Pd2 Y
• Calculated formula: C88 H90 Cl N4 O12 P4 Pd2 Y
• Title of publication: Stoichiometry controlled self-assembly of tri- and octa-nuclear palladium‒yttrium complexes
• Authors of publication: Chikkali, Samir H.; Nieger, Martin; Gudat, Dietrich
• Journal of publication: New Journal of Chemistry
• Year of publication: 2010
• Journal volume: 34
• Journal issue: 7
• Pages of publication: 1348
• a: 19.804 ± 0.004 Å
• b: 20.246 ± 0.004 Å
• c: 21.28 ± 0.004 Å
• α: 90°
• β: 98.08 ± 0.02°
• γ: 90°
• Cell volume: 8448 ± 3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.134
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1002
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No