Information card for entry 7053441

Structure parameters

• Common name: (mu4-hydroxo-octakis-(mu-3-3-(diphenyl)methyl-1,2- catecholato)-tetra-(dimethylformamide)-tetra-yttrium(iii)-tetra- palladium(ii))trichloride dimethylformamide solvate (penta)hydrate
• Chemical name: [mu4-hydroxo-octakis-(mu-3-3-(diphenyl)methyl-1,2-catecholato)-tetra- (dimethylformamide)-tetra-yttrium(III)-tetra-palladium(II)]trichloride dimethylformamide solvate (penta)hydrate
• Formula: C200 H243 Cl3 N16 O38 P8 Pd4 Y4
• Calculated formula: C200 H232 Cl3 N16 O38.001 P8 Pd4 Y4
• Title of publication: Stoichiometry controlled self-assembly of tri- and octa-nuclear palladium‒yttrium complexes
• Authors of publication: Chikkali, Samir H.; Nieger, Martin; Gudat, Dietrich
• Journal of publication: New Journal of Chemistry
• Year of publication: 2010
• Journal volume: 34
• Journal issue: 7
• Pages of publication: 1348
• a: 16.374 ± 0.0002 Å
• b: 18.8825 ± 0.0002 Å
• c: 20.612 ± 0.0003 Å
• α: 67.152 ± 0.001°
• β: 70.115 ± 0.001°
• γ: 74.181 ± 0.001°
• Cell volume: 5449.58 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1049
• Residual factor for significantly intense reflections: 0.0754
• Weighted residual factors for significantly intense reflections: 0.1931
• Weighted residual factors for all reflections included in the refinement: 0.2138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No