Information card for entry 7053462

Structure parameters

• Formula: C36 H39 Al Ge
• Calculated formula: C36 H39 Al Ge
• SMILES: [Ge]1(/C(=C\c2ccccc2)[Al]([C]1#Cc1ccccc1)(C(C)(C)C)C(C)(C)C)(c1ccccc1)c1ccccc1
• Title of publication: Hydroalumination of dialkynylgermanes—synthesis of alkenyl‒alkynylgermanes with intramolecular aluminium‒carbon interactions
• Authors of publication: Uhl, Werner; Rohling, Martina; Kösters, Jutta
• Journal of publication: New Journal of Chemistry
• Year of publication: 2010
• Journal volume: 34
• Journal issue: 8
• Pages of publication: 1630
• a: 8.4449 ± 0.0003 Å
• b: 9.9162 ± 0.0004 Å
• c: 20.1186 ± 0.0007 Å
• α: 87.777 ± 0.002°
• β: 87.692 ± 0.002°
• γ: 66.821 ± 0.002°
• Cell volume: 1547.02 ± 0.1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0413
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0954
• Weighted residual factors for all reflections included in the refinement: 0.0996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No