Information card for entry 7053463

Structure parameters

• Formula: C38 H43 Al Ge
• Calculated formula: C38 H43 Al Ge
• SMILES: [Ge]1(/C(=C\c2ccccc2)[Al]([C]1#Cc1ccccc1)(CC(C)(C)C)CC(C)(C)C)(c1ccccc1)c1ccccc1
• Title of publication: Hydroalumination of dialkynylgermanes—synthesis of alkenyl‒alkynylgermanes with intramolecular aluminium‒carbon interactions
• Authors of publication: Uhl, Werner; Rohling, Martina; Kösters, Jutta
• Journal of publication: New Journal of Chemistry
• Year of publication: 2010
• Journal volume: 34
• Journal issue: 8
• Pages of publication: 1630
• a: 10.0303 ± 0.0002 Å
• b: 30.7031 ± 0.0005 Å
• c: 10.9998 ± 0.0002 Å
• α: 90°
• β: 98.733 ± 0.001°
• γ: 90°
• Cell volume: 3348.24 ± 0.11 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0363
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0863
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No