Information card for entry 7102245

Structure parameters

• Formula: C39 H65.67 Al N2 O4 S Si
• Calculated formula: C38.9998 H65.6662 Al N2 O4 S Si
• Title of publication: Soluble, reactive and stable - unique aluminosilicate ligands and a heterobimetallic derivative [LAl(SLi)(micro-O)Si(OLi.2thf)(OtBu)2]2.
• Authors of publication: Jancik, Vojtech; Rascón-Cruz, Fernando; Cea-Olivares, Raymundo; Toscano, Rubén A
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 43
• Pages of publication: 4528 - 4530
• a: 31.536 ± 0.005 Å
• b: 31.536 ± 0.005 Å
• c: 22.246 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 19160 ± 6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1251
• Weighted residual factors for all reflections included in the refinement: 0.1388
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No