Information card for entry 7102246

Structure parameters

• Formula: C41 H69 Al N2 O6 Si
• Calculated formula: C41 H69 Al N2 O6 Si
• Title of publication: Soluble, reactive and stable - unique aluminosilicate ligands and a heterobimetallic derivative [LAl(SLi)(micro-O)Si(OLi.2thf)(OtBu)2]2.
• Authors of publication: Jancik, Vojtech; Rascón-Cruz, Fernando; Cea-Olivares, Raymundo; Toscano, Rubén A
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2007
• Journal issue: 43
• Pages of publication: 4528 - 4530
• a: 9.504 ± 0.001 Å
• b: 22.74 ± 0.002 Å
• c: 20.13 ± 0.002 Å
• α: 90°
• β: 90.87 ± 0.02°
• γ: 90°
• Cell volume: 4350 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0852
• Residual factor for significantly intense reflections: 0.0651
• Weighted residual factors for significantly intense reflections: 0.17
• Weighted residual factors for all reflections included in the refinement: 0.1846
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No