Information card for entry 7104428

Structure parameters

• Formula: Co6 H146 K3 Na21 O253 P6 W48
• Calculated formula: Co6 K2.1 Na8.1 O213.1 P6 W48
• Title of publication: The trinity of polyoxometalates: connecting {M12} Keggin and {M18} Dawson clusters to triangles.
• Authors of publication: Mitchell, Scott G; Khanra, Sumit; Miras, Haralampos N; Boyd, Thomas; Long, De-Liang; Cronin, Leroy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 19
• Pages of publication: 2712 - 2714
• a: 17.2294 ± 0.0002 Å
• b: 25.6034 ± 0.0004 Å
• c: 28.861 ± 0.0005 Å
• α: 79.469 ± 0.002°
• β: 87.59 ± 0.002°
• γ: 83.489 ± 0.002°
• Cell volume: 12433.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1668
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1543
• Weighted residual factors for all reflections included in the refinement: 0.196
• Goodness-of-fit parameter for all reflections included in the refinement: 0.873
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No