Information card for entry 7104449

Structure parameters

• Formula: C19 H47 I N4 O Si3 U
• Calculated formula: C19 H47 I N4 O Si3 U
• SMILES: [U]123(I)(N([Si](C)(C)C)CC[N]3(CCN1[Si](C)(C)C)CCN2[Si](C)(C)C)[O]1CCCC1
• Title of publication: Synthesis and structure of [{N(CH2CH2NSiMe3)3}URe(eta5-C5H5)2]: a heterobimetallic complex with an unsupported uranium-rhenium bond.
• Authors of publication: Gardner, Benedict M; McMaster, Jonathan; Lewis, William; Liddle, Stephen T
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 20
• Pages of publication: 2851 - 2853
• a: 12.8637 ± 0.0003 Å
• b: 12.8637 ± 0.0003 Å
• c: 36.191 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5988.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 96
• Hermann-Mauguin space group symbol: P 43 21 2
• Hall space group symbol: P 4nw 2abw
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for significantly intense reflections: 0.049
• Weighted residual factors for all reflections included in the refinement: 0.053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No