Information card for entry 7104450

Structure parameters

• Formula: C25 H49 N4 Re Si3 U
• Calculated formula: C25 H49 N4 Re Si3 U
• SMILES: [U]123(N([Si](C)(C)C)CC[N]2(CCN1[Si](C)(C)C)CCN3[Si](C)(C)C)[Re]12345678([cH]9[cH]4[cH]3[cH]2[cH]19)[cH]1[cH]5[cH]7[cH]8[cH]61
• Title of publication: Synthesis and structure of [{N(CH2CH2NSiMe3)3}URe(eta5-C5H5)2]: a heterobimetallic complex with an unsupported uranium-rhenium bond.
• Authors of publication: Gardner, Benedict M; McMaster, Jonathan; Lewis, William; Liddle, Stephen T
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 20
• Pages of publication: 2851 - 2853
• a: 15.805 ± 0.002 Å
• b: 10.2483 ± 0.0012 Å
• c: 19.91 ± 0.003 Å
• α: 90°
• β: 100.734 ± 0.002°
• γ: 90°
• Cell volume: 3168.5 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No