Crystallography Open Database

Information card for entry 7104958

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Structure parameters

Formula	C47 H68 Ge N4
Calculated formula	C47 H68 Ge N4
SMILES	[Ge]1(N(C(=C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C)=C1N(C(=C(N1C(C)C)C)C)C(C)C.Cc1ccccc1
Title of publication	From NHC‒>germylenes to stable NHC‒>germanone complexes.
Authors of publication	Yao, Shenglai; Xiong, Yun; Driess, Matthias
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2009
Journal issue	42
Pages of publication	6466 - 6468
a	11.1525 ± 0.0004 Å
b	14.2463 ± 0.0005 Å
c	14.3356 ± 0.0006 Å
α	74.438 ± 0.003°
β	80.643 ± 0.003°
γ	87.108 ± 0.003°
Cell volume	2164.92 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0789
Residual factor for significantly intense reflections	0.046
Weighted residual factors for significantly intense reflections	0.0704
Weighted residual factors for all reflections included in the refinement	0.076
Goodness-of-fit parameter for all reflections included in the refinement	0.942
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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