Information card for entry 7104959

Structure parameters

• Formula: C41 H64 Cl2 Ge N4 O2
• Calculated formula: C41 H64 Cl2 Ge N4 O2
• Title of publication: From NHC–>germylenes to stable NHC–>germanone complexes.
• Authors of publication: Yao, Shenglai; Xiong, Yun; Driess, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 6466 - 6468
• a: 11.6635 ± 0.0003 Å
• b: 24.5936 ± 0.0007 Å
• c: 15.6283 ± 0.0003 Å
• α: 90°
• β: 102.959 ± 0.002°
• γ: 90°
• Cell volume: 4368.76 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0918
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1584
• Weighted residual factors for all reflections included in the refinement: 0.1693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No