Information card for entry 7104960

Structure parameters

• Formula: C40 H60 Ge N4 O
• Calculated formula: C40 H60 Ge N4 O
• SMILES: [Ge]1(=O)(N(C(=C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C)=C1N(C(=C(N1C(C)C)C)C)C(C)C
• Title of publication: From NHC‒>germylenes to stable NHC‒>germanone complexes.
• Authors of publication: Yao, Shenglai; Xiong, Yun; Driess, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 6466 - 6468
• a: 21.2684 ± 0.0005 Å
• b: 16.941 ± 0.0004 Å
• c: 21.6339 ± 0.0005 Å
• α: 90°
• β: 94.333 ± 0.002°
• γ: 90°
• Cell volume: 7772.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0685
• Weighted residual factors for all reflections included in the refinement: 0.0757
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No