Information card for entry 7110914

Structure parameters

• Formula: C38.14 H40.28 Cl0.28 Ir N6 O2 Rh
• Calculated formula: C38.14 H40.28 Cl0.28 Ir N6 O2 Rh
• Title of publication: Redox-active heterobinuclear triazenide-bridged complexes; ancillary ligand control of electron distribution in a three-electron metal‒metal bond
• Authors of publication: Connelly, Neil G.; Hayward, Owen D.; Klangsinsirikul, Phimphaka; Orpen, A. Guy; Rieger, Philip H.
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 963
• a: 15.052 ± 0.004 Å
• b: 13.982 ± 0.002 Å
• c: 17.202 ± 0.003 Å
• α: 90 ± 0.013°
• β: 98.426 ± 0.014°
• γ: 90 ± 0.01°
• Cell volume: 3581.2 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.0882
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No