Electrophilic halogenation of thioethers: 5-chloro- and 5,6-dichloro-5,6-dihydro-1,3-dithiolo[4,5-b][1,4]dithiine-2-one and an efficient synthesis of vinylenedithiotetrathiafulvalene (VDT-TTF)
Authors of publication
Dautel, Olivier J.; Larsen, Jan; Fourmigué, Marc
Journal of publication
Chemical Communications
Year of publication
2000
Journal issue
13
Pages of publication
1117
a
6.4203 ± 0.0013 Å
b
14.905 ± 0.003 Å
c
11.648 ± 0.002 Å
α
90°
β
93.58 ± 0.03°
γ
90°
Cell volume
1112.5 ± 0.4 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
3
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0412
Residual factor for significantly intense reflections
0.0268
Weighted residual factors for significantly intense reflections
0.0565
Weighted residual factors for all reflections included in the refinement
0.059
Goodness-of-fit parameter for all reflections included in the refinement
