Information card for entry 7110924

Structure parameters

• Formula: C26 H48 Li4 N4 Si4
• Calculated formula: C26 H48 Li4 N4 Si4
• Title of publication: The arched four-rung ladder structure of the unsolvated dilithium salt of N,N′-bis(trimethylsilyl)-2-aminobenzylamine, and its structural deformation on THF complexation
• Authors of publication: Gauvin, Régis M.; Kress, Jacky; Kyritsakas, Nathalie; Fischer, Jean
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 965
• a: 9.759 ± 0.0002 Å
• b: 21.354 ± 0.0004 Å
• c: 16.794 ± 0.0006 Å
• α: 90°
• β: 98.073 ± 0.005°
• γ: 90°
• Cell volume: 3465.08 ± 0.16 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for all reflections: 0.292
• Weighted residual factors for all reflections included in the refinement: 0.058
• Goodness-of-fit parameter for all reflections: 5.653
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No