Information card for entry 7110925

Structure parameters

• Formula: C34 H64 Li4 N4 O2 Si4
• Calculated formula: C34 H58 Li4 N4 O2 Si4
• Title of publication: The arched four-rung ladder structure of the unsolvated dilithium salt of N,N′-bis(trimethylsilyl)-2-aminobenzylamine, and its structural deformation on THF complexation
• Authors of publication: Gauvin, Régis M.; Kress, Jacky; Kyritsakas, Nathalie; Fischer, Jean
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 965
• a: 19.9167 ± 0.0009 Å
• b: 9.8818 ± 0.0002 Å
• c: 22.1151 ± 0.0009 Å
• α: 90°
• β: 99.75 ± 0.002°
• γ: 90°
• Cell volume: 4289.7 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.102
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for all reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections: 1.58
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No