Information card for entry 7111046

Structure parameters

• Formula: C13 H39 Li N2 Si4 Zn
• Calculated formula: C13 H39 Li N2 Si4 Zn
• Title of publication: ‘Inverse crown ether’ complexes extended to group 12 through the syntheses of [Na2Zn2(HMDS)4(O)] and [{K2Zn2(HMDS)4(O2)x(O)y}∞]
• Authors of publication: Forbes, Glenn C.; Kennedy, Alan R.; Mulvey, Robert E.; Rowlings, René B.; Clegg, William; Liddle, Stephen T.; Wilson, Chick C.
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 18
• Pages of publication: 1759
• a: 17.04 ± 0.01 Å
• b: 6.84 ± 0.008 Å
• c: 21.558 ± 0.01 Å
• α: 90°
• β: 108.47 ± 0.04°
• γ: 90°
• Cell volume: 2383 ± 3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0593
• Weighted residual factors for significantly intense reflections: 0.1345
• Weighted residual factors for all reflections included in the refinement: 0.1441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No