Information card for entry 7111047

Structure parameters

• Formula: C24 H72 N4 Na2 O Si8 Zn2
• Calculated formula: C24 H72 N4 Na2 O Si8 Zn2
• SMILES: [Zn]12[O]34[Na]([N]1([Si](C)(C)C)[Si](C)(C)C)[N]([Zn]3[N]([Na]4[N]2([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C
• Title of publication: ‘Inverse crown ether’ complexes extended to group 12 through the syntheses of [Na2Zn2(HMDS)4(O)] and [{K2Zn2(HMDS)4(O2)x(O)y}∞ ]
• Authors of publication: Forbes, Glenn C.; Kennedy, Alan R.; Mulvey, Robert E.; Rowlings, René B.; Clegg, William; Liddle, Stephen T.; Wilson, Chick C.
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 18
• Pages of publication: 1759
• a: 10.711 ± 0.006 Å
• b: 12.81 ± 0.006 Å
• c: 8.97 ± 0.004 Å
• α: 108.96 ± 0.03°
• β: 99.77 ± 0.04°
• γ: 96.13 ± 0.04°
• Cell volume: 1129.7 ± 1 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.1231
• Weighted residual factors for all reflections included in the refinement: 0.1305
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No