Information card for entry 7111298

Structure parameters

• Formula: C90 H140 Al2 Li8 N6 O17
• Calculated formula: C90.008 H140 Al2 Li8 N6 O17
• Title of publication: Heterobimetallic lithium alkyltriimido aluminate cages containing the [R?Al(NR)3]4? tetraanion (R? = Bun, Et; R = 2-OMeC6H4)Electronic supplementary information (ESI) available: syntheses of 1?4. See http://www.rsc.org/suppdata/cc/b3/b307589c/
• Authors of publication: Copsey, May C.; Jeffery, John C.; Russell, Christopher A.; Slattery, John M.; Straughan, Jennifer A.
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2356
• a: 15.547 ± 0.003 Å
• b: 22.129 ± 0.004 Å
• c: 27.386 ± 0.006 Å
• α: 90°
• β: 101.84 ± 0.03°
• γ: 90°
• Cell volume: 9221 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0792
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1253
• Weighted residual factors for all reflections included in the refinement: 0.1405
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No