Information card for entry 7111299

Structure parameters

• Formula: C86 H132 Al2 Li8 N6 O15
• Calculated formula: C86 H132 Al2 Li8 N6 O15
• Title of publication: Heterobimetallic lithium alkyltriimido aluminate cages containing the [R?Al(NR)3]4? tetraanion (R? = Bun, Et; R = 2-OMeC6H4)Electronic supplementary information (ESI) available: syntheses of 1?4. See http://www.rsc.org/suppdata/cc/b3/b307589c/
• Authors of publication: Copsey, May C.; Jeffery, John C.; Russell, Christopher A.; Slattery, John M.; Straughan, Jennifer A.
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2356
• a: 18.2874 ± 0.0003 Å
• b: 20.0934 ± 0.0004 Å
• c: 24.9608 ± 0.0005 Å
• α: 90°
• β: 105.114 ± 0.001°
• γ: 90°
• Cell volume: 8854.7 ± 0.3 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.095
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.2047
• Weighted residual factors for all reflections included in the refinement: 0.2211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No