Information card for entry 7111408

Structure parameters

• Formula: C78 H66 O3 Pb2
• Calculated formula: C78 H54 O3 Pb2
• Title of publication: New Pb?Pb bonds: syntheses and molecular structures of hexabiphenyldiplumbane and tri(trisbiphenylplumbyl)plumbate
• Authors of publication: Wang, Yuzhong; Quillian, Brandon; Wei, Pingrong; Yang, Xiao-Juan; Robinson, Gregory H.
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 19
• Pages of publication: 2224 - 2225
• a: 11.943 ± 0.0019 Å
• b: 14.431 ± 0.002 Å
• c: 19.402 ± 0.003 Å
• α: 89.378 ± 0.003°
• β: 89.819 ± 0.004°
• γ: 70.374 ± 0.003°
• Cell volume: 3149.5 ± 0.8 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1101
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.107
• Weighted residual factors for all reflections included in the refinement: 0.1197
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No