Information card for entry 7111409

Structure parameters

• Formula: C148 H147 Cl3 Mg2 O7 Pb4
• Calculated formula: C148 H147 Cl3 Mg2 O7 Pb4
• SMILES: [Pb]([Pb](c1ccc(cc1)c1ccccc1)(c1ccc(cc1)c1ccccc1)c1ccc(cc1)c1ccccc1)([Pb](c1ccc(cc1)c1ccccc1)(c1ccc(cc1)c1ccccc1)c1ccc(cc1)c1ccccc1)[Pb](c1ccc(cc1)c1ccccc1)(c1ccc(cc1)c1ccccc1)c1ccc(cc1)c1ccccc1.c1(ccccc1)c1ccccc1.[Mg]12([Cl][Mg]([Cl]1)([Cl]2)([O]1CCCC1)([O]1CCCC1)[O]1CCCC1)([O]1CCCC1)([O]1CCCC1)[O]1CCCC1.O1CCCC1
• Title of publication: New Pb?Pb bonds: syntheses and molecular structures of hexabiphenyldiplumbane and tri(trisbiphenylplumbyl)plumbate
• Authors of publication: Wang, Yuzhong; Quillian, Brandon; Wei, Pingrong; Yang, Xiao-Juan; Robinson, Gregory H.
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 19
• Pages of publication: 2224 - 2225
• a: 19.222 ± 0.003 Å
• b: 19.329 ± 0.003 Å
• c: 20.958 ± 0.003 Å
• α: 77.52 ± 0.004°
• β: 85.906 ± 0.004°
• γ: 67.523 ± 0.003°
• Cell volume: 7024.7 ± 1.9 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1273
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.1231
• Weighted residual factors for all reflections included in the refinement: 0.1607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No