Information card for entry 7111439

Structure parameters

• Common name: 1,3-Di-tert.butyl-2-chloro-1,3,2-diazastibolenium tetrachloroantmonate
• Chemical name: 1,3-Di-tert.butyl-2-chloro-1,3,2-diazastibolenium tetrachloroantmonate
• Formula: C10 H20 Cl4 N2 Sb2
• Calculated formula: C10 H20 Cl4 N2 Sb2
• Title of publication: Synthesis and unprecedented oxidation of a cationic Sb-analogue of an Arduengo's carbene
• Authors of publication: Gudat, Dietrich; Gans-Eichler, Timo; Nieger, Martin
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 21
• Pages of publication: 2434 - 2435
• a: 10.1078 ± 0.0001 Å
• b: 19.52 ± 0.0002 Å
• c: 10.234 ± 0.0001 Å
• α: 90°
• β: 114.408 ± 0.001°
• γ: 90°
• Cell volume: 1838.75 ± 0.03 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0192
• Residual factor for significantly intense reflections: 0.018
• Weighted residual factors for significantly intense reflections: 0.0416
• Weighted residual factors for all reflections included in the refinement: 0.0419
• Goodness-of-fit parameter for all reflections included in the refinement: 1.214
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No