Information card for entry 7111440

Structure parameters

• Common name: N,N'-Di-tert.butyl-diazadiene antimopny trichloride, antimony trichloride adduct
• Chemical name: N,N'-Di-tert.butyl-diazadiene antimopny trichloride, antimony trichloride adduct
• Formula: C10 H20 Cl6 N2 Sb2
• Calculated formula: C10 H20 Cl6 N2 Sb2
• Title of publication: Synthesis and unprecedented oxidation of a cationic Sb-analogue of an Arduengo's carbene
• Authors of publication: Gudat, Dietrich; Gans-Eichler, Timo; Nieger, Martin
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 21
• Pages of publication: 2434 - 2435
• a: 12.0617 ± 0.0001 Å
• b: 17.4255 ± 0.0002 Å
• c: 19.3913 ± 0.0002 Å
• α: 90°
• β: 102.081 ± 0.001°
• γ: 90°
• Cell volume: 3985.42 ± 0.07 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0261
• Residual factor for significantly intense reflections: 0.0182
• Weighted residual factors for significantly intense reflections: 0.0391
• Weighted residual factors for all reflections included in the refinement: 0.0406
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No