Information card for entry 7113254

Structure parameters

• Formula: C20 H44.83 B11 Cl0.17 Rh2
• Calculated formula: C20 H44.83 B11 Cl0.17 Rh2
• Title of publication: Macropolyhedral boron-containing cluster chemistry. The unique nido-five-vertex-〈B2〉-nido-ten-vertex conjuncto structure of [(η5-C5Me5)2Rh2B11H15] via an unexpected cluster-dismantling
• Authors of publication: Carr, Michael J.; Perera, Sarath D.; Jelínek, Tomáš; Štíbr, Bohumil; Clegg, William; Kilner, Colin A.; Kennedy, John D.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 34
• Pages of publication: 3559 - 3561
• a: 8.8255 ± 0.0005 Å
• b: 9.9185 ± 0.0006 Å
• c: 17.9003 ± 0.001 Å
• α: 89.867 ± 0.001°
• β: 79.475 ± 0.001°
• γ: 68.194 ± 0.001°
• Cell volume: 1426.63 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.6932 Å
• Diffraction radiation type: synchrotron
• Duplicate of: 7102109
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No