Information card for entry 7113255

Structure parameters

• Formula: C20 H49 B16 Cl Rh2
• Calculated formula: C20 H49 B16 Cl Rh2
• Title of publication: Macropolyhedral boron-containing cluster chemistry. The unique nido-five-vertex-〈B2〉-nido-ten-vertex conjuncto structure of [(η5-C5Me5)2Rh2B11H15] via an unexpected cluster-dismantling
• Authors of publication: Carr, Michael J.; Perera, Sarath D.; Jelínek, Tomáš; Štíbr, Bohumil; Clegg, William; Kilner, Colin A.; Kennedy, John D.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 34
• Pages of publication: 3559 - 3561
• a: 11.4055 ± 0.0002 Å
• b: 10.4608 ± 0.0002 Å
• c: 14.3232 ± 0.0003 Å
• α: 90°
• β: 109.545 ± 0.001°
• γ: 90°
• Cell volume: 1610.44 ± 0.05 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0319
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0804
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7102110
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No