Information card for entry 7114267

Structure parameters

• Formula: C87 H71 N2 O2 P W
• Calculated formula: C87 H71 N2 O2 P W
• Title of publication: Formation of novel diaza-metallacycles by insertion of tungsten(ii) aryloxides into aromatic diazine ringsElectronic supplementary information (ESI) available: synthesis of compounds 1???4. See http://www.rsc.org/suppdata/cc/b2/b207805h/
• Authors of publication: Lentz, Margaret R.; Fanwick, Phillip E.; Rothwell, Ian P.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 2482
• a: 12.215 ± 0.0002 Å
• b: 32.4594 ± 0.0005 Å
• c: 17.0957 ± 0.0002 Å
• α: 90°
• β: 93.0186 ± 0.0009°
• γ: 90°
• Cell volume: 6768.9 ± 0.17 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for all reflections included in the refinement: 0.089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No