Information card for entry 7114268

Structure parameters

• Formula: C71 H57 N2 O2 P W
• Calculated formula: C71 H57 N2 O2 P W
• Title of publication: Formation of novel diaza-metallacycles by insertion of tungsten(ii) aryloxides into aromatic diazine ringsElectronic supplementary information (ESI) available: synthesis of compounds 1???4. See http://www.rsc.org/suppdata/cc/b2/b207805h/
• Authors of publication: Lentz, Margaret R.; Fanwick, Phillip E.; Rothwell, Ian P.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 2482
• a: 11.3255 ± 0.0001 Å
• b: 16.3547 ± 0.0003 Å
• c: 18.3239 ± 0.0003 Å
• α: 70.6136 ± 0.0007°
• β: 73.1055 ± 0.0006°
• γ: 71.1026 ± 0.0011°
• Cell volume: 2964.61 ± 0.08 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for all reflections included in the refinement: 0.085
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No