Information card for entry 7116916

Structure parameters

• Formula: C16 H14 Co2 O7
• Calculated formula: C16 H14 Co2 O7
• Title of publication: Expanding the scope of strained-alkyne chemistry: a protection-deprotection strategy via the formation of a dicobalt-hexacarbonyl complex
• Authors of publication: Pierangelo Gobbo; Tommaso Romagnoli; Stephanie M. Barbon; Jacquelyn T. Price; Jennifer Keir; Joe B. Gilroy; Mark S. Workentin
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 6647
• a: 8.893 ± 0.003 Å
• b: 16.495 ± 0.006 Å
• c: 19.797 ± 0.009 Å
• α: 101.28 ± 0.016°
• β: 102.13 ± 0.012°
• γ: 103.697 ± 0.012°
• Cell volume: 2664.8 ± 1.8 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0231
• Weighted residual factors for significantly intense reflections: 0.0571
• Weighted residual factors for all reflections included in the refinement: 0.06
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No