Crystallography Open Database

Information card for entry 7116917

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Coordinates	7116917.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H14 Co2 O7
Calculated formula	C16 H14 Co2 O7
Title of publication	Expanding the scope of strained-alkyne chemistry: a protection-deprotection strategy via the formation of a dicobalt-hexacarbonyl complex
Authors of publication	Pierangelo Gobbo; Tommaso Romagnoli; Stephanie M. Barbon; Jacquelyn T. Price; Jennifer Keir; Joe B. Gilroy; Mark S. Workentin
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	6647
a	9.074 ± 0.003 Å
b	12.983 ± 0.006 Å
c	16.699 ± 0.005 Å
α	110.879 ± 0.017°
β	96.205 ± 0.008°
γ	98.023 ± 0.009°
Cell volume	1793.4 ± 1.2 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.036
Residual factor for significantly intense reflections	0.0285
Weighted residual factors for significantly intense reflections	0.0668
Weighted residual factors for all reflections included in the refinement	0.0701
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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