Crystallography Open Database

Information card for entry 7116918

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Coordinates	7116918.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H17 Co2 N O11
Calculated formula	C23 H17 Co2 N O11
Title of publication	Expanding the scope of strained-alkyne chemistry: a protection-deprotection strategy via the formation of a dicobalt-hexacarbonyl complex
Authors of publication	Pierangelo Gobbo; Tommaso Romagnoli; Stephanie M. Barbon; Jacquelyn T. Price; Jennifer Keir; Joe B. Gilroy; Mark S. Workentin
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	6647
a	39.343 ± 0.02 Å
b	8.101 ± 0.004 Å
c	16.72 ± 0.006 Å
α	90°
β	110.966 ± 0.013°
γ	90°
Cell volume	4976 ± 4 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0672
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0636
Weighted residual factors for all reflections included in the refinement	0.0724
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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