Information card for entry 7117027

Structure parameters

• Common name: (PPh4)[Sn(N3)3]
• Chemical name: Tetraphenylphosphonium triazidostannate(II)
• Formula: C24 H20 N9 P Sn
• Calculated formula: C24 H20 N9 P Sn
• Title of publication: Homoleptic low-valent polyazides of group 14 elements
• Authors of publication: Benjamin Peerless; Theo Keane; Anthony J. H. M. Meijer; Peter Portius
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 7435
• a: 10.756 ± 0.0006 Å
• b: 11.0605 ± 0.0006 Å
• c: 12.354 ± 0.0007 Å
• α: 91.668 ± 0.004°
• β: 108.414 ± 0.004°
• γ: 116.545 ± 0.003°
• Cell volume: 1222.1 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0954
• Weighted residual factors for all reflections included in the refinement: 0.102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No