Information card for entry 7119225

Structure parameters

• Formula: C65.5 H108 Cl4 Ge2 N4 P4 Pd2
• Calculated formula: C65.5 H108 Cl4 Ge2 N4 P4 Pd2
• Title of publication: Synthesis and initial transition metal chemistry of the first PGeP pincer-type germylene.
• Authors of publication: Álvarez-Rodríguez, Lucía; Brugos, Javier; Cabeza, Javier A.; García-Álvarez, Pablo; Pérez-Carreño, Enrique; Polo, Diego
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 5
• Pages of publication: 893 - 896
• a: 11.7387 ± 0.0006 Å
• b: 17.267 ± 0.001 Å
• c: 18.6974 ± 0.001 Å
• α: 74.296 ± 0.005°
• β: 80.993 ± 0.004°
• γ: 80.308 ± 0.004°
• Cell volume: 3571.6 ± 0.3 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0318
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No