Information card for entry 7121301

Structure parameters

• Formula: C173 H163 Cl8 F12 N4 O18 P10 Pd4 S2
• Calculated formula: C173 H163 Cl8 F12 N4 O18 P10 Pd4 S2
• Title of publication: The chelate-to-bridging shift of phosphane dipalladacycles: convenient synthesis of double A-frame tetranuclear complexes.
• Authors of publication: Frieiro-Gomis, Pablo; Lucio-Martínez, Fátima; Munín-Cruz, Paula; Ortigueira, Juan M.; Pereira, M. Teresa; Polo-Ces, Paula; Vázquez-García, Digna; Vila, José M
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 21
• Pages of publication: 2662 - 2665
• a: 14.8431 ± 0.0011 Å
• b: 26.413 ± 0.002 Å
• c: 22.3504 ± 0.0019 Å
• α: 90°
• β: 93.09 ± 0.006°
• γ: 90°
• Cell volume: 8749.8 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1533
• Residual factor for significantly intense reflections: 0.0773
• Weighted residual factors for significantly intense reflections: 0.195
• Weighted residual factors for all reflections included in the refinement: 0.257
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No