Information card for entry 7121302

Structure parameters

• Formula: C176 H172 Cl2 F12 N4 O20 P10 Pd4
• Calculated formula: C176 H172 Cl2 F12 N4 O20 P10 Pd4
• Title of publication: The chelate-to-bridging shift of phosphane dipalladacycles: convenient synthesis of double A-frame tetranuclear complexes.
• Authors of publication: Frieiro-Gomis, Pablo; Lucio-Martínez, Fátima; Munín-Cruz, Paula; Ortigueira, Juan M.; Pereira, M. Teresa; Polo-Ces, Paula; Vázquez-García, Digna; Vila, José M
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 21
• Pages of publication: 2662 - 2665
• a: 16.4987 ± 0.0006 Å
• b: 16.5332 ± 0.0006 Å
• c: 17.1548 ± 0.0005 Å
• α: 82.897 ± 0.002°
• β: 71.882 ± 0.002°
• γ: 75.24 ± 0.002°
• Cell volume: 4295.6 ± 0.3 ų
• Cell temperature: 97 ± 2 K
• Ambient diffraction temperature: 97 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1292
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No