Information card for entry 7121321

Structure parameters

• Formula: C36 H52 N2 P Sb
• Calculated formula: C36 H52 N2 P Sb
• Title of publication: Phosphaalkene-substituted organo-group 15 compounds: synthesis and characterisation of (NHC)P-EtBu₂ (E = P, As, Sb and Bi).
• Authors of publication: Balmer, Markus; Gottschling, Hannah; von Hänisch, Carsten
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 21
• Pages of publication: 2659 - 2661
• a: 9.5816 ± 0.0005 Å
• b: 11.7784 ± 0.0007 Å
• c: 16.7485 ± 0.0009 Å
• α: 88.332 ± 0.002°
• β: 80.966 ± 0.003°
• γ: 70.456 ± 0.002°
• Cell volume: 1758.61 ± 0.17 ų
• Cell temperature: 100.01 K
• Ambient diffraction temperature: 100.01 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0515
• Weighted residual factors for all reflections included in the refinement: 0.0544
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No