Information card for entry 7121322

Structure parameters

• Formula: C29 H44 Bi N2 P
• Calculated formula: C29 H44 Bi N2 P
• Title of publication: Phosphaalkene-substituted organo-group 15 compounds: synthesis and characterisation of (NHC)P-EtBu₂ (E = P, As, Sb and Bi).
• Authors of publication: Balmer, Markus; Gottschling, Hannah; von Hänisch, Carsten
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 21
• Pages of publication: 2659 - 2661
• a: 8.5219 ± 0.0007 Å
• b: 10.0762 ± 0.0008 Å
• c: 37.319 ± 0.003 Å
• α: 85.58 ± 0.002°
• β: 87.36 ± 0.003°
• γ: 68.332 ± 0.002°
• Cell volume: 2968.7 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1003
• Weighted residual factors for all reflections included in the refinement: 0.1046
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No