Information card for entry 7121453

Structure parameters

• Formula: C103.5 H144 N8 P4 Sm2
• Calculated formula: C103.5 H144 N8 P4 Sm2
• Title of publication: Reactivity of bulky Ln(ii) amidinates towards P₄, As₄, and As₄S₄.
• Authors of publication: Schoo, Christoph; Bestgen, Sebastian; Köppe, Ralf; Konchenko, Serygey N.; Roesky, Peter W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 38
• Pages of publication: 4770 - 4773
• a: 14.1425 ± 0.0002 Å
• b: 14.9026 ± 0.0002 Å
• c: 26.1273 ± 0.0004 Å
• α: 98.343 ± 0.001°
• β: 96.438 ± 0.001°
• γ: 111.506 ± 0.001°
• Cell volume: 4986.58 ± 0.13 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0284
• Weighted residual factors for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections included in the refinement: 0.0737
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No