Information card for entry 7121454

Structure parameters

• Formula: C54 H78 As N4 O S2 Sm
• Calculated formula: C54 H78 As N4 O S2 Sm
• Title of publication: Reactivity of bulky Ln(ii) amidinates towards P₄, As₄, and As₄S₄.
• Authors of publication: Schoo, Christoph; Bestgen, Sebastian; Köppe, Ralf; Konchenko, Serygey N.; Roesky, Peter W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 38
• Pages of publication: 4770 - 4773
• a: 14.6528 ± 0.0008 Å
• b: 17.1717 ± 0.0007 Å
• c: 21.7016 ± 0.0011 Å
• α: 90°
• β: 96.826 ± 0.004°
• γ: 90°
• Cell volume: 5421.7 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0896
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0495
• Weighted residual factors for all reflections included in the refinement: 0.0557
• Goodness-of-fit parameter for all reflections included in the refinement: 0.904
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No