Information card for entry 7121456

Structure parameters

• Formula: C54 H78 As N4 O S2 Yb
• Calculated formula: C54 H78 As N4 O S2 Yb
• Title of publication: Reactivity of bulky Ln(ii) amidinates towards P₄, As₄, and As₄S₄.
• Authors of publication: Schoo, Christoph; Bestgen, Sebastian; Köppe, Ralf; Konchenko, Serygey N.; Roesky, Peter W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 38
• Pages of publication: 4770 - 4773
• a: 14.5485 ± 0.0016 Å
• b: 17.054 ± 0.0007 Å
• c: 21.7258 ± 0.0015 Å
• α: 90°
• β: 96.905 ± 0.007°
• γ: 90°
• Cell volume: 5351.3 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0237
• Weighted residual factors for significantly intense reflections: 0.0309
• Weighted residual factors for all reflections included in the refinement: 0.0326
• Goodness-of-fit parameter for all reflections included in the refinement: 0.933
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No