Crystallography Open Database

Information card for entry 7121455

Preview

Coordinates	7121455.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C100 H140 As4 N8 Sm2
Calculated formula	C100 H140 As4 N8 Sm2
Title of publication	Reactivity of bulky Ln(ii) amidinates towards P<sub>4</sub>, As<sub>4</sub>, and As<sub>4</sub>S<sub>4</sub>.
Authors of publication	Schoo, Christoph; Bestgen, Sebastian; Köppe, Ralf; Konchenko, Serygey N.; Roesky, Peter W.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	38
Pages of publication	4770 - 4773
a	13.6808 ± 0.0007 Å
b	16.1681 ± 0.0008 Å
c	22.4917 ± 0.0011 Å
α	99.664 ± 0.004°
β	94.939 ± 0.004°
γ	95.996 ± 0.004°
Cell volume	4850.2 ± 0.4 Å³
Cell temperature	110 K
Ambient diffraction temperature	108 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1106
Residual factor for significantly intense reflections	0.0642
Weighted residual factors for significantly intense reflections	0.1527
Weighted residual factors for all reflections included in the refinement	0.1755
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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